Mass spectrometry, Edexcel As chemistry 5 main steps of a mass spectrometer 2.5 / 5 based on 6 ratings ? ChemistrySpectroscopyASEdexcel Created on: 04-04-12 15:53 what can we use it for? it can be used for determining 1. Relative atomic mass 2. Relative molecular mass 3. Isotopic abundance 4. Molecular structure 1 of 7 Steps 1 .Vaporisation 2. Ionisation 3. Accelration 4. Deflection 5. Detection Remember: Vanessa is a dandy dancer. 2 of 7 Vaporisation The sample is turned into GAS aka... vaporised! this is done by using an electrical heater. 3 of 7 Ionisation The gas particles are bombarded with high speed electrons and this ionises them the electrons knock off other electrons in order to form positive ions 4 of 7 Acceleration the positive ions are accelerated by an electric field 5 of 7 Deflection the positive ions' paths changes with a magnetic field. the lighter ions have less momentun and are deflected more easily than heavier ions. for a given magnetic field. only ions with a particular M/Z ( mass / charge ) ratio make it to the detector. 6 of 7 Deflection the magnetic field strength is slowly increased. this changed the mass/charge ratio of ions that can reach the detector. this produces a mass spectrum 7 of 7
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