stages in the laboratory preparation of ethyl ethanoate
Ethyl ethanoate (ethyl acetate) is an ester. The equation for preparing an ester is: ‘acid + alcohol → ester + water’ (reversible reaction).
Ethanoic acid + ethanol ethyl ethanoate + water
Safety: - Goggles - Gloves - Fume Cupboard - Lab Coat
1) Place ethanol and pure ethanoic acid into a round bottomed flask with sulfuric acid (catalyst- speeds up reaction) then heat under reflux condenser so the liquid doesn't evaporate.
2) Distil off the ester with a condenser so the impure product is separated from the reaction mixture after refluxing.
3) Use a separating funnel to shake the impure ester with aqueous reagents (sodium carbonate) to remove impurities. The ester layer can be tapped off from the separating funnel for purification.
4) The drying agent (anhydrous calcium carbonate) helps to remove more impurities.
5) Bumping granules help mixture boil smoothly.Use distillation to ensure a pure dried ester is formed.
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